Hebrews 3:8

if ye will hear his voice, harden not your hearts, as in the provocation, in the day of temptation in the wilderness,

Hebrews 3:15

we hold fast the beginning of our confidence firm to the end) While it is said; To-day, if ye will hear his voice, harden not your hearts, as in the provocation.

Revelation 16:9

And the men were scorched exceedingly, and blasphemed the name of God, who had power over these plagues: but they repented not to give him glory.

Treasury of Scripture Knowledge

Summary

But when Pharaoh saw that there was respite, he hardened his heart, and hearkened not unto them; as the LORD had said.

Bible References

He hardened

Hebrews 3:8
if ye will hear his voice, harden not your hearts, as in the provocation, in the day of temptation in the wilderness,
Revelation 16:9
And the men were scorched exceedingly, and blasphemed the name of God, who had power over these plagues: but they repented not to give him glory.