Exodus 9:24

And there was hail, and fire [was] flashing back and forth in the midst of the very severe hail, the like of which was not in all the land of Egypt since it had become a nation.

Exodus 9:23

And Moses stretched out his staff to the heavens, and Yahweh gave thunder and hail, and fire went [to the] earth, and Yahweh caused hail to rain on the land of Egypt.

Exodus 10:6

And your houses will be full, and the houses of all your servants and the houses of all Egypt, [something] that your fathers and {your grandfathers} never saw from the day they were on the earth until this day.'" And he turned and went out from Pharaoh.

Matthew 24:21

For at that time there will be great tribulation, such as has not happened from the beginning of the world until now, nor ever will happen.

Treasury of Scripture Knowledge

Summary

So there was hail, and fire mingled with the hail, very grievous, such as there was none like it in all the land of Egypt since it became a nation.

General references

Bible References

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Exodus 9:23
And Moses stretched out his staff to the heavens, and Yahweh gave thunder and hail, and fire went [to the] earth, and Yahweh caused hail to rain on the land of Egypt.
Exodus 10:6
And your houses will be full, and the houses of all your servants and the houses of all Egypt, [something] that your fathers and {your grandfathers} never saw from the day they were on the earth until this day.'" And he turned and went out from Pharaoh.
Matthew 24:21
For at that time there will be great tribulation, such as has not happened from the beginning of the world until now, nor ever will happen.

General references

Job 38:23
which I have reserved for [the] time of trouble, for [the] day of battle and war?